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Why electron-beam
imaging?
Simple gravimetric
(e.g., weighing) methods have long been used to assess the total
mass of particulate material, and flow-counter instruments are widely
used to obtain distributions of particles by number and average
size.
But for truly accurate assessment of unknown or variable particle
populations, only direct particle-by-particle imaging provides sufficiently
detailed knowledge for meaningful characterization. Fortunately,
such microscopic examination can today be conducted by automated
microscopes from easily prepared filter samples. However, light-based
(optical) microscopes are severely limited in their ability to characterize
particle populations accurately. Fortunately, there is a superior
alternative available; electron-beam imaging provides demonstrable
advantages in the critical areas of:
• Magnification
• Contrast mechanisms
• Depth of focus
• Dynamic control
• Elemental composition
The
first four factors alone have repeatedly proved to establish the superiority
of electron-beam imaging for accurate and reliable quantification
of the sizes and shapes of both fine and coarse particles. And, surprisingly
to many, a well-engineered electron-beam tool is comparable in cost
and ease of use with a similarly automated light-based system. But,
for many applications, it is the unique capability of electron-beam
technology to unambiguously characterize inorganic particles by their
elemental composition that provides the definitive advantage over
all other methods.
There are many useful techniques available for inferring selected
parameters of particle distributions, but when reliable characterization
of particle populations by either morphology or composition is essential,
electron-beam imaging is the clear choice.
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